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Lab Exercise: Advanced Reporting
Performance Reports (System Suitability)
128
Select System Suitability from the Report menu, followed by Edit Noise
Ranges.
10) Examine prior chromatograms and select several time ranges for the noise
calculation. The ranges should be greater than one minute in duration in a
region where there are no chromatographic peaks. Fill in the table and OK
the dialog box.
11) Now, go to the Report menu and select Specify Report or use the Specify
Report tool.
Select an Extended Performance Report Style. OK the dialog box and
resave the method. Resave Quant.m.
12) Return to the Method and Run Control view. A complete system suitability
report cannot be printed from previously acquired data unless the column
information (void time) was filled in prior to the actual data acquisition. Turn
on the pump and lamp. Equilibrate the column. Make certain that the
method loaded is Quant.M. Under Method, RunTime Checklist, make
certain that both Data Acquisition and Data Analysis are selected.
13) From the RunControl menu, select Setup Sample Info. Give this data file
the name, syss.d. Set up the autosampler to inject one of the standards or the
original test mix. Run the Method.
14) Wait for the report to print and examine the report. Note the < or > sign that
appears when the calculated values exceed the specified limits.
Note: The equations for each performance test can be found in your manual,
Understanding Your ChemStation.
15) Return to the Data Analysis window. Under Report, select Specify Report.
Now select Performance + Noise as the Report style. Resave the method
and print the report.
- Agilent 1100/1200 HPLC 1
- ChemStation Operation 1
- Course Number H4033A 3
- Laboratory Manual 3
- Table Of Contents 5
- ChemStation 9
- In this Laboratory You Will: 10
- Configuration Editor 13
- Scheduler 14
- Windows XP) 16
- Cleaning up Temporary Files 16
- Repairing the Disk 16
- Disk Defragmentation 17
- Workstation) 18
- (Windows 2000 or XP) 21
- Windows Explorer 21
- Wallpaper and Screen Savers 22
- Clipboard 23
- Preparation 27
- Preparing the HPLC 28
- Practice Entering Gradients 32
- OK the dialog box 34
- Snapshot 35
- Graphics - Signal Options 39
- Graphics - Annotation 41
- Window Functions 43
- Peak Purity 44
- Displaying Spectra 47
- Isoabsorbance Plot 48
- 3D Plot 50
- Building a Library 53
- Library Searching 55
- The Agilent 1200 Flow Path 59
- Diagnosis View 61
- Diagnosis Instrument Panel 62
- Instrument Tests 64
- Routine Maintenance 67
- Agilent LC Diagnostic Tool 73
- Diagnosing Common Problems 74
- Instrument Status Report 77
- Lab Exercise: Integration 81
- Integration Preparation 83
- Auto Integration 84
- Adding Timed Events 87
- Using Manual Events 89
- Data Acquisition-Standards 97
- Integration 99
- Setting up Signal Details 101
- Building a Calibration Table 102
- Calibration Standards 104
- Building a Sequence 109
- Sequence Summary Reports 112
- Starting the Sequence 113
- Pausing a Sequence 114
- Post Sequence 115
- Reprocessing 117
- Reprocess with DA Methods 125
- Batch Review 129
- Adding a Report Header 133
- Automated Peak Purity 137
- Preparations 143
- Building a Customized Report 144
- Adding a General Section 145
- Inserting Tables 146
- Adding a Calibration Curve 147
- Finishing Up 148
- Lab Exercise: Commands 149
- In this LaboratoryYou Will: 150
- Commands 152
- Registers 153
- Objects 154
- Lab Exercise: Macro Writing 161
- Write Your Own Macro 165
- Possible Answer 166
- Agilent ChemStation 168
- Getting Started with New 168
- ChemStation Workflow 168
- In This Guide… 170
- 4 Data Organization 171
- Contents 172
- 6 Data Organization 173
- ChemStation Data Structure 174
- ChemStation prior to B.02.01 175
- ChemStation B.02.01/B.03.01 176
- 12 Data Organization 179
- 1 ChemStation Data Structure 179
- Data Acquisition 180
- 18 Data Organization 185
- 2 Data Acquisition 185
- Data Analysis 186
- 22 Data Organization 189
- 3 Data Analysis 189
- B.02.01 and higher 189
- Data Analysis: Data Review 190
- Keep “Current Method” 191
- Load “Sequence Method” 192
- Update master method feature 196
- Update Sequence Method 197
- Master method — 197
- Data Organization 33 200
- Data Analysis 3 200
- 34 Data Organization 201
- Agilent Technologies 202
- 42 Data Organization 209
- *G2170-90041* 211
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