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Lab Exercise: Introduction to the HPLC ChemStation
Maintaining the Windows XP Workstation
11
3) Click on the Tools tab. Find the Error-Checking tool and click Check
Now....
4) Select to Automatically fix file system errors and Scan for and attempt
recovery of bad sectors.
5) This process can take several minutes. If you don’t wish to do this in lab,
Cancel, otherwise select Start.
Disk Defragmentation
A defragmentation utility is included with Windows XP. Several vendors sell this
utility as well such as DiskKeeper. Make certain you defragment your disk drives
on a periodic basis. You must close all programs before beginning. The process
can take a long time. We will not do this here.
Creating an Emergency Repair Disk
You should create an emergency repair disk as soon as possible. Use this disk if
your system files are damaged or your computer won't start. The disk includes
system settings such as registry files, disk partitions, and installed devices. Make
a new repair disk every time you make changes to your hardware or software.
Emergency Repair Disks are specific for each computer. The backup process for
Windows XP goes farther than Windows 2000. It consists of two of two parts: a
backup file, and a Recovery Disk. The backup file will be large (we cannot do
this here), and the Recovery Disk will be a floppy.
1) From the Start button, select All Programs, Accessories, System Tools, then
Backup.
2) The Backup Utility Wizard should start by default unless it is disabled. If the
Wizard has been disabled, select Tools then Switch to Wizard Mode.
3) Click the Advanced Mode button found in the text.
4) Click the Automated System Recovery Wizard button.
5) Click Next>. The Wizard will start and prompt you for the media to use for
the backup file. As we don’t have the proper media here, cancel out.
You can write this file to a tape drive, a hard disk or writeable CD or DVD. After
entering the destination for the backup file, click Next> again, and finally, Finish.
The Windows XP Backup utility will copy all important system files and settings
to the backup file. An estimate and status bar are provided. After this step is
- Agilent 1100/1200 HPLC 1
- ChemStation Operation 1
- Course Number H4033A 3
- Laboratory Manual 3
- Table Of Contents 5
- ChemStation 9
- In this Laboratory You Will: 10
- Configuration Editor 13
- Scheduler 14
- Windows XP) 16
- Cleaning up Temporary Files 16
- Repairing the Disk 16
- Disk Defragmentation 17
- Workstation) 18
- (Windows 2000 or XP) 21
- Windows Explorer 21
- Wallpaper and Screen Savers 22
- Clipboard 23
- Preparation 27
- Preparing the HPLC 28
- Practice Entering Gradients 32
- OK the dialog box 34
- Snapshot 35
- Graphics - Signal Options 39
- Graphics - Annotation 41
- Window Functions 43
- Peak Purity 44
- Displaying Spectra 47
- Isoabsorbance Plot 48
- 3D Plot 50
- Building a Library 53
- Library Searching 55
- The Agilent 1200 Flow Path 59
- Diagnosis View 61
- Diagnosis Instrument Panel 62
- Instrument Tests 64
- Routine Maintenance 67
- Agilent LC Diagnostic Tool 73
- Diagnosing Common Problems 74
- Instrument Status Report 77
- Lab Exercise: Integration 81
- Integration Preparation 83
- Auto Integration 84
- Adding Timed Events 87
- Using Manual Events 89
- Data Acquisition-Standards 97
- Integration 99
- Setting up Signal Details 101
- Building a Calibration Table 102
- Calibration Standards 104
- Building a Sequence 109
- Sequence Summary Reports 112
- Starting the Sequence 113
- Pausing a Sequence 114
- Post Sequence 115
- Reprocessing 117
- Reprocess with DA Methods 125
- Batch Review 129
- Adding a Report Header 133
- Automated Peak Purity 137
- Preparations 143
- Building a Customized Report 144
- Adding a General Section 145
- Inserting Tables 146
- Adding a Calibration Curve 147
- Finishing Up 148
- Lab Exercise: Commands 149
- In this LaboratoryYou Will: 150
- Commands 152
- Registers 153
- Objects 154
- Lab Exercise: Macro Writing 161
- Write Your Own Macro 165
- Possible Answer 166
- Agilent ChemStation 168
- Getting Started with New 168
- ChemStation Workflow 168
- In This Guide… 170
- 4 Data Organization 171
- Contents 172
- 6 Data Organization 173
- ChemStation Data Structure 174
- ChemStation prior to B.02.01 175
- ChemStation B.02.01/B.03.01 176
- 12 Data Organization 179
- 1 ChemStation Data Structure 179
- Data Acquisition 180
- 18 Data Organization 185
- 2 Data Acquisition 185
- Data Analysis 186
- 22 Data Organization 189
- 3 Data Analysis 189
- B.02.01 and higher 189
- Data Analysis: Data Review 190
- Keep “Current Method” 191
- Load “Sequence Method” 192
- Update master method feature 196
- Update Sequence Method 197
- Master method — 197
- Data Organization 33 200
- Data Analysis 3 200
- 34 Data Organization 201
- Agilent Technologies 202
- 42 Data Organization 209
- *G2170-90041* 211
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